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    Experimental Determination of NH3 Solubility in Toluene at Pressures up to 340 kPa at 398 K

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    Date
    2014
    Author
    BHATTACHARYYA, SC
    PANT, CS
    MEHRA, A
    BHATTACHARYA, B
    MALIK, RK
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    Abstract
    The solubility of ammonia in toluene has been measured at 398 K and at pressures up to 340 kPa using a static, synthetic and isochoric technique. The goal of the present study is to determine the equilibrium solubility of ammonia in toluene at a pressure and temperature regime that is relevant to the reaction conditions of amination of 1,3,5-trichloro-2,4,6-trinitrobenzene leading to the formation of 1,3,5-triamino-2,4,6-trinitro benzene. The ammonia solubility data in toluene were hitherto unavailable under these experimental conditions. The solubility data have also been compared with the result obtained from a direct sampling method. The results are in agreement with Krichevsky-Kasarnovsky equation. The Henry's law constant at the reaction temperature has been determined.
    URI
    http://dx.doi.org/10.1007/s10953-014-0215-y
    http://dspace.library.iitb.ac.in/jspui/handle/100/16760
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