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| Title: | Characterization and conformational studies of a novel trinitro steroid using 2D-NMR |
| Authors: | KATOCH, R
SRIDHARAN, R
TRIVEDI, GK |
| Keywords: | nuclear-magnetic-resonance
fast atom bombardment
mass-spectrometry
ion-source
solids |
| Issue Date: | 1998 |
| Publisher: | INDIAN CHEMICAL SOC |
| Citation: | JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 75(10-12), 543-547 |
| Abstract: | Conformational analysis of nitro substituted 4-en-3-one steroids has been further investigated using high resolution 2D-NMR techniques. An attempt on the preparation of 6 beta-nitrocholest-4-en-3-one resulted in a new trinitro steroid, 2,2,6 beta-trinitrocholest-4-en-3-one. These compounds have been characterized using COSY, HETCOR, NOESY experiments and the probable pathways to these products have been discussed. |
| URI: | http://dspace.library.iitb.ac.in/xmlui/handle/10054/8767
http://hdl.handle.net/10054/8767 |
| ISSN: | 0019-4522 |
| Appears in Collections: | Article
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