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Please use this identifier to cite or link to this item: http://dspace.library.iitb.ac.in/jspui/handle/10054/12017

Title: Hexaacetato derivative of calix(6)arene for the solvent extraction separation of lead(II)
Authors: MALKHEDE, DD
PHADKE, M
DHADKE, PM
KHOPKAR, SM
Keywords: eosin
Issue Date: 1998
Publisher: SPECTROSCOPY SOC CANADA, OTTAWA
Citation: CANADIAN JOURNAL OF ANALYTICAL SCIENCES AND SPECTROSCOPY, 43(5), 144-148
Abstract: Lead(ll) was quantitatively extracted with 1 x 10(.4) M Calix(6)arene hexaacetato derivative in xylene at pH 6.0 with 4 M nitric acid. It was stripped and determined spectrophotometrically at 520 nm using 4-(2-pyridylazo) resorcinol. Although silver, indium and palladium showed strong interference, metals like molybdenum, selenium, chromium, tellurium associated in. minerals or tin, antimony, zinc, bismuth, thallium associated in, low fusible alloys are tolerated in the ratio 1:10. Anions, alkali and alkaline earths are well tolerated. The method was applied for determination of lead in, real samples like a solder. The reproducibility, expressed as Relative Standard Deviation is +/- 1.2%.
URI: http://dspace.library.iitb.ac.in/xmlui/handle/10054/12017
http://hdl.handle.net/10054/12017
ISSN: 1205-6685
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