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Please use this identifier to cite or link to this item: http://dspace.library.iitb.ac.in/jspui/handle/10054/10156

Title: STRUCTURE OF AN INTERMEDIATE METHYLATED PRODUCT IN THE SYNTHESIS OF DRIMANES
Authors: DAS, K
SINHA, UC
DESAI, SR
BHAT, SV
TAVALE, SS
PURANAIK, VG
Issue Date: 1992
Publisher: MUNKSGAARD INT PUBL LTD
Citation: ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 48(), 525-527
Abstract: 5-Methoxymethyl-1,1,4a-trimethyl-6-[(phenylthio)methyl]-1,5,8,8a-tetrahydro-4(4aH)-naphthalenone, C22H28O2S, m.p. = 382 K, M(r) = 356.53, monoclinic, P2(1)/c, a = 11.810 (1), b = 8.929 (2), c = 18.716 (1) angstrom, beta = 92.773 (8)-degrees, V = 1971.32 angstrom 3, Z = 4, D(x) = 1.201 Mg m-3, lambda(Mo K-alpha) = 0.71069 angstrom, mu(Mo K-alpha) = 0.137 mm-1, F(000) = 768, T = 291 K, final R = 0.055, wR = 0.074 using 2674 reflections. The bicyclic skeleton of the molecule is cis fused. An intermolecular C-H...O interaction [C(20)-H(20)...O(1') 3.306 (3) angstrom] was observed.
URI: http://dx.doi.org/10.1107/S0108270191009873
http://dspace.library.iitb.ac.in/xmlui/handle/10054/10156
http://hdl.handle.net/10054/10156
ISSN: 0108-2701
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